Effect of 1-deoxy-d-lactose upon the crystallization of D-lactose

Kevin P. Guiry; Simon J. Coles; Humphrey A. Moynihan; Simon E. Lawrence

doi:10.1021/cg070598n

Effect of 1-deoxy-d-lactose upon the crystallization of D-lactose

Kevin P. Guiry
, Simon J. Coles
, Humphrey A. Moynihan
, Simon E. Lawrence

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

The synthesis and crystal structure of 1-deoxy-D-lactose is described, as is its use as an additive in the crystallization of D-lactose. This has resulted in the formation of αβ-D-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.

Original language	English
Pages (from-to)	3927-3934
Number of pages	8
Journal	Crystal Growth and Design
Volume	8
Issue number	11
DOIs	https://doi.org/10.1021/cg070598n
Publication status	Published - Nov 2008

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10.1021/cg070598n

https://hdl.handle.net/10468/1421Licence: CC BY-NC-ND

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title = "Effect of 1-deoxy-d-lactose upon the crystallization of D-lactose",

abstract = "The synthesis and crystal structure of 1-deoxy-D-lactose is described, as is its use as an additive in the crystallization of D-lactose. This has resulted in the formation of αβ-D-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.",

author = "Guiry, \{Kevin P.\} and Coles, \{Simon J.\} and Moynihan, \{Humphrey A.\} and Lawrence, \{Simon E.\}",

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AU - Guiry, Kevin P.

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AU - Moynihan, Humphrey A.

AU - Lawrence, Simon E.

PY - 2008/11

Y1 - 2008/11

N2 - The synthesis and crystal structure of 1-deoxy-D-lactose is described, as is its use as an additive in the crystallization of D-lactose. This has resulted in the formation of αβ-D-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.

AB - The synthesis and crystal structure of 1-deoxy-D-lactose is described, as is its use as an additive in the crystallization of D-lactose. This has resulted in the formation of αβ-D-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.

UR - https://www.scopus.com/pages/publications/61549096227

U2 - 10.1021/cg070598n

DO - 10.1021/cg070598n

M3 - Article

AN - SCOPUS:61549096227

SN - 1528-7483

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SP - 3927

EP - 3934

JO - Crystal Growth and Design

JF - Crystal Growth and Design

IS - 11

ER -

Effect of 1-deoxy-d-lactose upon the crystallization of D-lactose

Abstract

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