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Gold sensitized sprayed SnO2 nanostructured film for enhanced LPG sensing

  • Umesh T. Nakate
  • , Pramila Patil
  • , Balaji G. Ghule
  • , Satish Ekar
  • , Ahmed Al-Osta
  • , V. V. Jadhav
  • , Rajaram S. Mane
  • , S. N. Kale
  • , Mu Naushad
  • , Colm O'Dwyer
  • Defence Research and Development Organisation India
  • Swami Ramanand Teerth Marathwada University
  • Defence Bioengineering and Electromedical Laboratory
  • Udgir
  • King Saud University

Research output: Contribution to journalArticlepeer-review

Abstract

We report LPG sensing of gold (Au)-sensitized SnO2 nanostructured film fabricated by an easy spray pyrolysis deposition method whose surface morphology is confirmed by field-emission scanning electron microscopy and atomic force microscopy images and structure by X-ray diffraction pattern. Energy dispersive X-ray spectrometer analysis has carried out for finding elemental composition. The SnO2 film is uniform and consists of spherical particles of ∼10 nm. The highest gas response observed at 780 ppm LPG concentration for pristine SnO2 is 28%, at operating temperature 623 K, which is greatly improved on Au sensitization up to 57% with 60 s rapid response time at 598 K operating temperarture. The high gas response is due to electronic effect and catalytic spill-over effect of Au sensitization. The improved sensing mechanism has throughly been explored.

Original languageEnglish
Pages (from-to)362-368
Number of pages7
JournalJournal of Analytical and Applied Pyrolysis
Volume124
DOIs
Publication statusPublished - 1 Mar 2017

Keywords

  • Gold sensitization
  • LPG
  • Nanostructure
  • SnO
  • Spray pyrolysis

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