Optimisation of the arc-discharge production of multi-walled carbon nanotubes

  • M. Cadek
  • , R. Murphy
  • , B. McCarthy
  • , A. Drury
  • , B. Lahr
  • , R. C. Barklie
  • , M. In Het Panhuis
  • , J. N. Coleman
  • , W. J. Blau

Research output: Contribution to journalArticlepeer-review

Abstract

The effect of varying current density and pressure during arc generation on the yield and purity of multi-walled nanotube-containing carbon soot has been studied in this work. Various soots were produced and characterised qualitatively using transmission electron microscopy and quantitatively using electron paramagnetic resonance and thermogravimetric analysis. It was found that both yield and purity increase as current density and pressure are increased to the limit of our experimental investigations, i.e. 195 A/cm2 and 500 Torr of helium. Under these conditions a yield of 24 mg/min soot containing 48% by mass nanotubes was obtained.

Original languageEnglish
Pages (from-to)923-928
Number of pages6
JournalCarbon
Volume40
Issue number6
DOIs
Publication statusPublished - May 2002
Externally publishedYes

Keywords

  • A. Carbon nanotubes
  • B. Arc discharge
  • C. Electron paramagnetic resonance
  • D. Carbon yield

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