Pilot-scale production and physicochemical characterisation of spray-dried nanoparticulated whey protein powders

Jacob R. Guralnick; Ram R. Panthi; Francesca Bot; Valeria L. Cenini; Barry M.G. O’Hagan; Shane V. Crowley; James A. O’Mahony

doi:10.1111/1471-0307.12797

Pilot-scale production and physicochemical characterisation of spray-dried nanoparticulated whey protein powders

Jacob R. Guralnick
, Ram R. Panthi
, Francesca Bot
, Valeria L. Cenini
, Barry M.G. O’Hagan
, Shane V. Crowley
, James A. O’Mahony

School of Food and Nutritional Sciences

Research output: Contribution to journal › Article › peer-review

Abstract

Spray-dried whey protein isolate (WPI) powders were prepared at pilot-scale from solutions without heat (WPI_UH), heated (WPI_H) or heated with calcium (WPI_HCa), which were analysed and compared with a control sample (WPI_C). WPI_C, WPI_UH, WPI_H and WPI_HCa solutions had whey protein denaturation levels of 0.0, 3.2, 64.4 and 74.4%, respectively. Computerised tomography scanning showed that 52.6_, 84.0, 74.5 and 41.9% of WPI_C, WPI_UH, WPI_H and WPI_HCa powder particles had diameters of ≤30 µm. WPI_HCa and WPI_H powders were cohesive, while WPI_C and WPI_UH powders were easy flowing. Marked differences in microstructure were observed between WPI_H and WPI_HCa. There were no measured differences in wall friction, bulk density or colour.

Original language	English
Pages (from-to)	581-591
Number of pages	11
Journal	International Journal of Dairy Technology
Volume	74
Issue number	3
DOIs	https://doi.org/10.1111/1471-0307.12797
Publication status	Published - Aug 2021

Keywords

Aggregation
Nanoparticles
Physical properties
Powder
Whey protein

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10.1111/1471-0307.12797

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@article{11fbc30f94174d74bd5bf716fed0c655,

title = "Pilot-scale production and physicochemical characterisation of spray-dried nanoparticulated whey protein powders",

abstract = "Spray-dried whey protein isolate (WPI) powders were prepared at pilot-scale from solutions without heat (WPIUH), heated (WPIH) or heated with calcium (WPIHCa), which were analysed and compared with a control sample (WPIC). WPIC, WPIUH, WPIH and WPIHCa solutions had whey protein denaturation levels of 0.0, 3.2, 64.4 and 74.4\%, respectively. Computerised tomography scanning showed that 52.6, 84.0, 74.5 and 41.9\% of WPIC, WPIUH, WPIH and WPIHCa powder particles had diameters of ≤30 µm. WPIHCa and WPIH powders were cohesive, while WPIC and WPIUH powders were easy flowing. Marked differences in microstructure were observed between WPIH and WPIHCa. There were no measured differences in wall friction, bulk density or colour.",

keywords = "Aggregation, Nanoparticles, Physical properties, Powder, Whey protein",

author = "Guralnick, \{Jacob R.\} and Panthi, \{Ram R.\} and Francesca Bot and Cenini, \{Valeria L.\} and O{\textquoteright}Hagan, \{Barry M.G.\} and Crowley, \{Shane V.\} and O{\textquoteright}Mahony, \{James A.\}",

note = "Publisher Copyright: {\textcopyright} 2021 The Authors. International Journal of Dairy Technology published by John Wiley \& Sons Ltd on behalf of Society of Dairy Technology",

year = "2021",

month = aug,

doi = "10.1111/1471-0307.12797",

language = "English",

volume = "74",

pages = "581--591",

journal = "International Journal of Dairy Technology",

issn = "1364-727X",

publisher = "Wiley-Blackwell",

number = "3",

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TY - JOUR

T1 - Pilot-scale production and physicochemical characterisation of spray-dried nanoparticulated whey protein powders

AU - Guralnick, Jacob R.

AU - Panthi, Ram R.

AU - Bot, Francesca

AU - Cenini, Valeria L.

AU - O’Hagan, Barry M.G.

AU - Crowley, Shane V.

AU - O’Mahony, James A.

PY - 2021/8

Y1 - 2021/8

N2 - Spray-dried whey protein isolate (WPI) powders were prepared at pilot-scale from solutions without heat (WPIUH), heated (WPIH) or heated with calcium (WPIHCa), which were analysed and compared with a control sample (WPIC). WPIC, WPIUH, WPIH and WPIHCa solutions had whey protein denaturation levels of 0.0, 3.2, 64.4 and 74.4%, respectively. Computerised tomography scanning showed that 52.6, 84.0, 74.5 and 41.9% of WPIC, WPIUH, WPIH and WPIHCa powder particles had diameters of ≤30 µm. WPIHCa and WPIH powders were cohesive, while WPIC and WPIUH powders were easy flowing. Marked differences in microstructure were observed between WPIH and WPIHCa. There were no measured differences in wall friction, bulk density or colour.

AB - Spray-dried whey protein isolate (WPI) powders were prepared at pilot-scale from solutions without heat (WPIUH), heated (WPIH) or heated with calcium (WPIHCa), which were analysed and compared with a control sample (WPIC). WPIC, WPIUH, WPIH and WPIHCa solutions had whey protein denaturation levels of 0.0, 3.2, 64.4 and 74.4%, respectively. Computerised tomography scanning showed that 52.6, 84.0, 74.5 and 41.9% of WPIC, WPIUH, WPIH and WPIHCa powder particles had diameters of ≤30 µm. WPIHCa and WPIH powders were cohesive, while WPIC and WPIUH powders were easy flowing. Marked differences in microstructure were observed between WPIH and WPIHCa. There were no measured differences in wall friction, bulk density or colour.

KW - Aggregation

KW - Nanoparticles

KW - Physical properties

KW - Powder

KW - Whey protein

UR - https://www.scopus.com/pages/publications/85107495524

U2 - 10.1111/1471-0307.12797

DO - 10.1111/1471-0307.12797

M3 - Article

AN - SCOPUS:85107495524

SN - 1364-727X

VL - 74

SP - 581

EP - 591

JO - International Journal of Dairy Technology

JF - International Journal of Dairy Technology

IS - 3

ER -

Pilot-scale production and physicochemical characterisation of spray-dried nanoparticulated whey protein powders

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Keywords

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